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ASTM D 1266 Document Information:
Title
Standard Test Method for Sulfur in Petroleum Products (Lamp Method)
ASTM International
Publication Date:
Dec 1, 2007
Scope:
This test method covers the determination of total sulfur in
liquid petroleum products in concentrations from 0.01 to 0.4 mass %
(Note 1). A special sulfate analysis procedure is described in
Annex A1 that permits the determination of sulfur in concentrations
as low as 5 mg/kg.
NOTE 1—The comparable lamp method for the determination of
sulfur in liquefied petroleum gas is described in Test Method D
2784. For the determination of sulfur in heavier petroleum products
that cannot be burned in a lamp, see the bomb method (Test Method D
129) the quartz tube method (IP 63), or the high-temperature method
(Test Method D 1552).
The direct burning procedure (Section 9) is applicable to the
analysis of such materials as gasoline, kerosine, naphtha, and
other liquids that can be burned completely in a wick lamp. The
blending procedure (Section 10) is applicable to the analysis of
gas oils and distillate fuel oils, naphthenic acids, alkyl phenols,
high sulfur content petroleum products, and many other materials
that cannot be burned satisfactorily by the direct burning
procedure.
Phosphorus compounds normally present in commercial gasoline do
not interfere. A correction is given for the small amount of acid
resulting from the combustion of the lead anti-knock fluids in
gasolines. Appreciable concentrations of acid-forming or
base-forming elements from other sources interfere when the
titration procedure is employed since no correction is provided in
these cases.
The values stated in SI units are to be regarded as standard. No
other units of measurement are included in this standard.
This standard does not purport to address all of the safety
concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and
health practices and determine the applicability of regulatory
limitations prior to use.
*A Summary of Changes section appears at the end of this
standard.
Keywords:
- lamp
- sulfur
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